Department of Chemistry, Shahid-Bahonar University of Kerman, Kerman, Iran. (P.O. Box 76169-133).
10.7508/ijnd.2014.04.013
Abstract
A novel complex of cadmium (II) [CdL0.5(NO3)(H2O)](1), L= N,N-bis (O-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. Compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by IR, 1HNMR spectroscopy, X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The gray single crystal of compound 1 has been synthesized by slow evaporation and characterized by IR, 1HNMR spectroscopy. Then, Compound 1 in nano size was used as initial reagent to obtain nano-particles of cadmium (II) oxide at 673 K by direct calcination. The obtained CdO nano-particles were characterized by XRD pattern as well as SEM images.
Rashidi Ranjbar, Z., Sheikhshoaie, I., & Bagheri, Z. (2014). Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet. International Journal of Nano Dimension, 5(Issue 4), 409-413. doi: 10.7508/ijnd.2014.04.013
MLA
Z. Rashidi Ranjbar; I. Sheikhshoaie; Z. Bagheri. "Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet". International Journal of Nano Dimension, 5, Issue 4, 2014, 409-413. doi: 10.7508/ijnd.2014.04.013
HARVARD
Rashidi Ranjbar, Z., Sheikhshoaie, I., Bagheri, Z. (2014). 'Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet', International Journal of Nano Dimension, 5(Issue 4), pp. 409-413. doi: 10.7508/ijnd.2014.04.013
VANCOUVER
Rashidi Ranjbar, Z., Sheikhshoaie, I., Bagheri, Z. Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet. International Journal of Nano Dimension, 2014; 5(Issue 4): 409-413. doi: 10.7508/ijnd.2014.04.013
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